제주대학교 Repository

Pt Dendrite Oxide Probe에 코팅된 전도성 고분자를 기반으로 한 pH & Glucose 센서 제작

Metadata Downloads
Abstract
We report pH and glucose sensors using the conducting polymer coated-Pt dendrite oxide probe. Scanning Electron Microscopy (SEM) and X-ray photoelectron Spectroscopy (XPS) were employed to characterize the structural and morphological features of electrodeposited dendrite layer. The conductive polymer pH sensor was worked in the range of pH 3~13. The calibration plots exhibited a Nernst behavior (slope:-59.2mV/pH) in the buffer solution. Additionally, the potentiometric analysis of glucose through monitoring pH change was performed, which was enzymatically generated on the sensor at the range from 0.5mM to 10mM with a sensitivity of 6.138±0.4348mV/mM. In real blood sample analysis, the glucose concentration in human blood was found to be 4.901±0.6338
Author(s)
정지영
Issued Date
2013
Awarded Date
2013. 2
Type
Dissertation
URI
http://dcoll.jejunu.ac.kr/jsp/common/DcLoOrgPer.jsp?sItemId=000000006265
Alternative Author(s)
Jeong,Ji Young
Affiliation
제주대학교 대학원
Department
대학원 화학과
Advisor
김덕수
Table Of Contents
Ⅰ. 서 론 1
Ⅱ. 실 험 8
Ⅱ-1. 시약 및 용액 제조 8
Ⅱ-2. 측정기기 9
Ⅱ-3. 전극 9
Ⅱ-4. Pt dendrite 전극의 제작 11
Ⅱ-5. GOD/TTBA/Pt dendrite Ox 전극 제작 13
Ⅱ-6. Potentiometric 검출 원리 16
Ⅲ. 결과 및 고찰 18
Ⅲ-1. Pt dendrite 형상 관찰 및 특성 분석 18
Ⅲ-1-1. SEM 분석 18
Ⅲ-1-2. XPS 분석 23
Ⅲ-2. Pt dendrite, TTBA pH 반응 실험 26
Ⅲ-3. 재현성 및 안정성 실험 31
Ⅲ-4. 최적화 실험 33
Ⅲ-5. Glucose 검정 곡선 37
Ⅲ-6. 혈액 분석 40
Ⅳ. 결론 43
Ⅴ. 참고 문헌 45
Abstract 49
Degree
Master
Publisher
제주대학교
Citation
정지영. (2013). Pt Dendrite Oxide Probe에 코팅된 전도성 고분자를 기반으로 한 pH & Glucose 센서 제작
Appears in Collections:
General Graduate School > Chemistry
공개 및 라이선스
  • 공개 구분공개
파일 목록

Items in Repository are protected by copyright, with all rights reserved, unless otherwise indicated.