Pt Dendrite Oxide Probe에 코팅된 전도성 고분자를 기반으로 한 pH & Glucose 센서 제작
- Abstract
- We report pH and glucose sensors using the conducting polymer coated-Pt dendrite oxide probe. Scanning Electron Microscopy (SEM) and X-ray photoelectron Spectroscopy (XPS) were employed to characterize the structural and morphological features of electrodeposited dendrite layer. The conductive polymer pH sensor was worked in the range of pH 3~13. The calibration plots exhibited a Nernst behavior (slope:-59.2mV/pH) in the buffer solution. Additionally, the potentiometric analysis of glucose through monitoring pH change was performed, which was enzymatically generated on the sensor at the range from 0.5mM to 10mM with a sensitivity of 6.138±0.4348mV/mM. In real blood sample analysis, the glucose concentration in human blood was found to be 4.901±0.6338
- Author(s)
- 정지영
- Issued Date
- 2013
- Awarded Date
- 2013. 2
- Type
- Dissertation
- URI
- http://dcoll.jejunu.ac.kr/jsp/common/DcLoOrgPer.jsp?sItemId=000000006265
- Alternative Author(s)
- Jeong,Ji Young
- Affiliation
- 제주대학교 대학원
- Department
- 대학원 화학과
- Advisor
- 김덕수
- Table Of Contents
- Ⅰ. 서 론 1
Ⅱ. 실 험 8
Ⅱ-1. 시약 및 용액 제조 8
Ⅱ-2. 측정기기 9
Ⅱ-3. 전극 9
Ⅱ-4. Pt dendrite 전극의 제작 11
Ⅱ-5. GOD/TTBA/Pt dendrite Ox 전극 제작 13
Ⅱ-6. Potentiometric 검출 원리 16
Ⅲ. 결과 및 고찰 18
Ⅲ-1. Pt dendrite 형상 관찰 및 특성 분석 18
Ⅲ-1-1. SEM 분석 18
Ⅲ-1-2. XPS 분석 23
Ⅲ-2. Pt dendrite, TTBA pH 반응 실험 26
Ⅲ-3. 재현성 및 안정성 실험 31
Ⅲ-4. 최적화 실험 33
Ⅲ-5. Glucose 검정 곡선 37
Ⅲ-6. 혈액 분석 40
Ⅳ. 결론 43
Ⅴ. 참고 문헌 45
Abstract 49
- Degree
- Master
- Publisher
- 제주대학교
- Citation
- 정지영. (2013). Pt Dendrite Oxide Probe에 코팅된 전도성 고분자를 기반으로 한 pH & Glucose 센서 제작
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- General Graduate School > Chemistry
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